GDW-106 Oyile Dew Point Tester
●Le miyalelo ilandelayo isetyenziswa ngumntu oqeqeshiweyo ukunqanda ukothuka kombane.Sukwenza nayiphi na inkonzo engaphaya kwemiyalelo yokusebenza ngaphandle kokuba ufanelekile ukwenza njalo.
●Musa ukusebenzisa esi sixhobo kwindawo enokutsha nefumileyo.Gcina ubuso bucocekile kwaye bomile.
●Nceda uqinisekise ukuba isixhobo sime nkqo phambi kokuba uvule.Musa ukuwisa izixhobo kakhulu kuthintele umonakalo intshukumo isixhobo.
●Beka izixhobo kwindawo eyomileyo, ecocekileyo, nengenamoya ongena gesi engcolisayo.Ukupakisha izixhobo ngaphandle kwezikhongozeli zokuhamba kuyingozi.
●Iphaneli kufuneka ime nkqo ngexesha lokugcinwa.Phakamisa izinto ezigciniweyo ukukhusela kubumanzi.
●Musa ukuqhawula isixhobo ngaphandle kwemvume, eya kuchaphazela iwaranti yemveliso.Umzi-mveliso awunaxanduva lokuzidiliza ngokwawo.
Ixesha lewaranti yolu chungechunge ngunyaka OWONYE ukususela kumhla wokuthunyelwa, nceda ubhekisele kwi-invoyisi yakho okanye amaxwebhu okuthumela ukuze ubone imihla efanelekileyo yewaranti.I-HVHIPOT iqinisekisa umthengi wokuqala ukuba le mveliso ayinaziphene kwizinto eziphathekayo kunye nokusebenza phantsi kokusetyenziswa okuqhelekileyo.Ngalo lonke ixesha lewaranti, ukubonelela ukuba ezo ziphene azigqitywanga yi-HVHIPOT ukuba ibangelwa ukusetyenziswa kakubi, ukusetyenziswa kakubi, ukuguqulwa, ukufakela okungafanelekanga, ukungahoywa okanye imeko embi yendalo, i-HVHIPOT inqunyelwe kuphela ukulungisa okanye ukutshintshwa kwesi sixhobo ngexesha lewaranti.
| Hayi. | Igama | Qty. | Iyunithi |
| 1 | GDW-106 Umamkeli | 1 | iqhekeza |
| 2 | Ibhotile yeseli ye-Electrolytic | 1 | iqhekeza |
| 3 | Electrolytic electrode | 1 | iqhekeza |
| 4 | I-electrode yokulinganisa | 1 | iqhekeza |
| 5 | Electrolytic cell injection plug | 1 | iqhekeza |
| 6 | Iplagi enkulu yokugaya iglasi | 1 | iqhekeza |
| 7 | Iplagi yokusila yeglasi encinci (inotshi) | 1 | iqhekeza |
| 8 | Iplagi yokugaya iglasi encinci | 1 | iqhekeza |
| 9 | Ukubetha intonga | 2 | iipcs |
| 10 | Amasuntswana ejeli yesilika | 1 | ibhegi |
| 11 | I-silica gel pad | 9 | iipcs |
| 12 | 0.5μl isampulu encinci | 1 | iqhekeza |
| 13 | 50μl isampulu encinci | 1 | iqhekeza |
| 14 | 1ml isampula encinci | 1 | iqhekeza |
| 15 | Umbhobho owomileyo othe ngqo | 1 | iqhekeza |
| 16 | Ikhodi yamandla | 1 | iqhekeza |
| 17 | Vacuum igrisi | 1 | iqhekeza |
| 18 | Electrolyte | 1 | Ibhotile |
| 19 | Iphepha lokuprinta | 1 | roll |
| 20 | Isikhokelo somsebenzisi | 1 | iqhekeza |
| 21 | Ingxelo yovavanyo | 1 | iqhekeza |
HV Hipot Electric Co., Ltd. uye ngokungqongqo nangokucokisekileyo proofread manual, kodwa asinakuqinisekisa ukuba akukho ziphoso kunye nokukhutshwa ngokupheleleyo kwincwadana.
I-HV Hipot Electric Co., Ltd. izimisele ukwenza uphuculo oluqhubekayo kwimisebenzi yemveliso, kunye nokuphucula umgangatho wenkonzo, ngoko ke inkampani ihlala inelungelo lokutshintsha naziphi na iimveliso kunye neenkqubo zesofthiwe ezichazwe kule ncwadana kunye nomxholo wale ncwadana isaziso.
Itekhnoloji yeCoulometric Karl Fischer isetyenziswa ukulinganisa ngokuchanekileyo ukulandelela ukufuma kwisampulu elinganisiweyo.Itekhnoloji isetyenziswa ngokubanzi ukuchaneka kunye neendleko zovavanyo ezitshiphu.Imodeli ye-GDW-106 yokulinganisa ilandelela ngokuchanekileyo ukufuma kwiisampuli zolwelo, eziqinileyo kunye negesi ngokwetekhnoloji.Isetyenziselwa umbane, i-petroleum, iikhemikhali, ukutya njalo njalo.
Esi sixhobo sisebenzisa iiyunithi zokusetyenzwa kwesizukulwana esitsha esinamandla kunye nesekethe entsha ye-peripheral kunye nokuba ukusetyenziswa kwamandla aphantsi aphezulu kuyenza ikwazi ukusebenzisa ibhetri yokugcina encinci kwaye iphathekayo.Ukugweba i-electrolysis endpoint isekelwe kuvavanyo lwesignali ye-electrode kunye nokuzinza kunye nokuchaneka zizinto ezibalulekileyo zokuchaneka kokuzimisela.
●I-5-inch high-definition color touch screen, umboniso ucacile kwaye kulula ukuwusebenzisa.
●Iindlela ezimbini zembuyekezo ye-electrolyte engenanto yangoku kunye ne-balance point drift imbuyekezo ukuhlaziya iziphumo zovavanyo.
●Imisebenzi yokufumanisa i-electrode yokulinganisa impazamo yesiphaluka evulekileyo kunye nephutha lesiphaluka esifutshane.
●Yamkela umshicileli omncinci we-thermal, ukuprinta kulula kwaye kuyakhawuleza.
●Iifomula zokubala ezi-5 zakhiwe kwisixhobo, kwaye iyunithi yokubala yeziphumo zovavanyo (mg / L, ppm%) inokukhethwa njengoko ifunwa.
●Gcina iirekhodi zembali ngokuzenzekelayo ngethebhu yexesha, ubuninzi beerekhodi ezingama-500.
●I-microprocessor yangoku engenanto ilawula ngokuzenzekelayo imbuyekezo, kwaye ii-reagents zinokufikelela ngokukhawuleza kwi-equilibrium.
●Uluhlu lokulinganisa: 0ug-100mg;
●Ukuchaneka komlinganiselo:
Electrolysis amanzi Ukuchaneka
3ug-1000ug ≤±2ug
>1000ug ≤±02% (ezi parameters zingentla azibandakanyi impazamo yokutofa)
●Isigqibo: 0.1ug;
●Electrolyzing yangoku: 0-400mA;
●Ukusetyenziswa kwamandla aphezulu: 20W;
●Ukufakwa kwamandla: AC230V ± 20%, 50Hz ± 10%;
●Ubushushu bokusebenza kwi-Ambient: 5～40℃;
●Ukufuma okuSebenzayo kwi-Ambient: ≤85%
●Ubungakanani: 330×240×160mm
●Ubunzima obuninzi: 6kg.
Ulwakhiwo lweSixhobo kunye neNdibano
1. Umamkeli
Umfanekiso 4-1 Umamkeli
2. Iseli ye-Electrolytic
Umfanekiso we-4-2 umzobo wokubola kweseli ye-Electrolytic
Umzobo 4-3 umzobo wendibano yeseli ye-Electrolytic
1.I-electrode yokulinganisa i-electrode 2. I-electrode yokulinganisa ilothe 3. Electrolytic electrode 4. Electrolytic electrode lead 5. Ion filter membrane 6. Ukomisa iplagi yokusila ityhubhu yeglasi 7. Ityhubhu yokomisa 8. I-allochroic silicagel (i-drying agent) 9. Isampuli yokungena 10. Stirrer 111 Stirre .Anode chamber 12. Cathode chamber 13. Electrolytic cell glass grinding plug
●Beka iinqununu ze-silicone eluhlaza okwesibhakabhaka (i-agent yokomisa) kwi-tube yokumisa (i-7 kwi-Fig. 4-2).
Qaphela: Umbhobho wombhobho wokumisa kufuneka ugcine umoya othile wokungena emoyeni kwaye awukwazi ukutywinwa ngokupheleleyo, ngaphandle koko kulula ukubangela ingozi!
●Faka i-silicone pad emhlophe emhlophe kwiqhude kwaye uyijike ngokulinganayo kunye nezikhonkwane zokuqinisa (jonga umfanekiso 4-4).
Umzobo 4-4 umzobo wendibano yeplagi yokutofa
●Ngononophelo beka i-stirrer kwibhotile ye-electrolytic ngokusebenzisa isampuli yokungena.
●Usasaza ngokulinganayo umaleko wegrisi yokufunxa kwi-electrode yokulinganisa, i-electrolytic electrode, ityhubhu yokomisa igumbi lecathode, kunye nezibuko lokusila inkuku.Emva kokufaka amacandelo angentla kwibhotile ye-electrolytic, yijikeleze ngobumnene ukuze ivalwe ngcono.
●Malunga ne-120-150 ml ye-electrolyte itofwa kwigumbi le-anode yeseli ye-electrolytic ukusuka kwizibuko lokutywina iseli ye-electrolytic kunye nefaneli ecocekileyo neyomileyo (okanye kusetyenziswa isitshintshi solwelo), kwaye ifakwe kwakhona kwigumbi le-anode yeseli ye-electrolytic ukusuka i-electrolytic electrode seal port yi-funnel (okanye usebenzisa i-liquid change), ukwenza inqanaba le-electrolyte ngaphakathi kwegumbi le-cathode kunye ne-anode yegumbi yinto efanayo.Emva kokugqiba, iplagi yokugaya iglasi yeseli ye-electrolytic ifakwe ngokulinganayo kunye ne-vacuum grease kwaye ifakwe kwindawo ehambelana nayo, ijikelezwe ngobunono ukuze itywinwe ngcono.
Qaphela: Umsebenzi wokulayisha i-electrolyte ungentla kufuneka wenziwe kwindawo engena umoya.Musa ukuphefumla okanye ubambe ii-reagents ngesandla.Ukuba ithe yadibana nolusu, yihlambe ngamanzi.
Emva kokugqiba la manyathelo angentla, faka iseli ye-electrolytic kwinkxaso yeseli ye-electrolytic (9 kwi-Fig. 4-1), faka ucingo lokudibanisa i-electrolytic electrode kunye neplagi ye-lotus kunye nentambo yokudibanisa i-electrode kwi-interface ye-electrolytic electrode ( 7 kumfanekiso. 4-1).) kunye ne-electrode interface yokulinganisa (8 kwi-Fig.4-1).
Isisombululo se-reagent ngumxube we-iodine, i-pyridine egcwele i-sulfur dioxide kunye ne-methanol.Umgaqo wokuphendula we-Karl-Fischer reagent ngamanzi: ngokusekelwe kubukho bamanzi, iodine iyancitshiswa yi-sulfure dioxide, kwaye phambi kwe-pyridine kunye ne-methanol, i-pyridine hydroiodide kunye ne-methyl hydrogen hydrogen pyridine yenziwe.Indlela yokusabela yile:
H20+I2+SO2+3C5H5N → 2C5H5N·HI+C5H5N·SO3 …………(1)
C5H5N·SO3+CH3OH → C5H5N·HSO4CH3 ……………………(2)
Ngexesha lenkqubo ye-electrolysis, i-electrode reaction ilandelayo:
I-Anode: 2I- - 2e → I2 ..........................................(3)
I-Cathode: 2H+ + 2e → H2↑..............................................(4)
I-iodine eveliswa yi-anode iphendula ngamanzi ukuze yenze i-hydroiodic acid de kube kugqitywe ukuphendulwa kwawo onke amanzi, kwaye isiphelo sokuphendula siboniswa yiyunithi yokufumanisa eyenziwe nge-electrode yeplatinum.Ngokomthetho kaFaraday we-electrolysis, inani leemolekyuli ze-iodine ezithatha inxaxheba ekuphenduleni zilingana nenani leemolekyuli zamanzi, ezilingana nomlinganiselo wentlawulo yombane.Ubungakanani bamanzi kunye nentlawulo ineequation ilandelayo:
W=Q/10.722 ……………………………………………… (5)
W--ubumanzi umxholo weSampuli yeYunithi: ug
Q-ubungakanani bombane wentlawulo yombane: mC
Isixhobo samkela i-LCD yesikrini esikhulu, kwaye ubuninzi bolwazi olunokuthi luboniswe kwisikrini ngasinye lucebile, olunciphisa inani lokutshintsha izikrini.Ngamaqhosha okuchukumisa, imisebenzi yamaqhosha ichazwe ngokucacileyo, kulula ukuyisebenzisa.
Isixhobo sahlulwe kwizikrini ezi-5 zokubonisa:
●Boot isikrini sokwamkela;
●Ixesha lokucwangcisa isikrini;
●Isikrini sedatha yembali;
●Isikrini sovavanyo lwesampula;
●Isikrini sesiphumo somlinganiselo;
1. I-Boot Welcome Screen
Qhagamshela intambo yamandla esixhobo kwaye uvule iswitshi yamandla.Isikrini se-LCD sibonisa njengoko kubonisiwe kuMfanekiso 6-1:
2.Time Setting Screen
Cinezela iqhosha elithi "Ixesha" kumzobo we-Figure 6-1, kwaye isikrini se-LCD siya kubonisa njengoko kubonisiwe kuMfanekiso 6-2:
Kolu jongano, cofa inani lexesha okanye umhla wemizuzwana emi-3 ukuseta okanye ukulinganisa ixesha kunye nomhla.
Cinezela
isitshixo umva kujongano lokuqala.
3. Isikrini seDatha yeMbali
Cinezela iqhosha elithi "Data" kwisikrini soMfanekiso 6-1, kwaye isikrini se-LCD siya kubonisa njengoko kubonisiwe kuMfanekiso 6-3:
Cinezela
isitshixo sokutshintsha amaphepha.
Cinezela
Isitshixo sokucima idatha yangoku.
Cinezela
iqhosha lokuprinta idatha yangoku.
Cinezelaisitshixo umva kujongano lokuqala.
4. Isikrini sovavanyo lwesampula
Cinezela iqhosha elithi "Vavanya" kwisikrini soMfanekiso 6-1, isikrini se-LCD siya kubonisa njengoko kubonisiwe ngezantsi:
Ukuba i-electrolyte kwiseli ye-electrolytic isanda kutshintshwa, imeko yangoku iya kubonisa "I-Reagent phezu kwe-iodine, nceda ugcwalise ngamanzi".Emva kokucofa ngokucofa ukutofa amanzi kwigumbi le-anode kunye nesampulu ye-50ul de i-electrolyte ijike ibe tyheli, imeko yangoku iya kubonisa "Nceda ulinde", kwaye isixhobo siya kulungelelanisa ngokuzenzekelayo.
Ukuba i-electrolyte kwiseli ye-electrolytic isetyenzisiwe, imeko yangoku iya kubonisa "Nceda ulinde", kwaye isixhobo siya kulungelelanisa ngokuzenzekelayo.
I-pre-conditioning iqala, oko kukuthi isitya se-titration ayomiswa."Nceda ulinde" iya kubonisa, isixhobo esizenzekelayo sibhala amanzi angaphezulu.
Cinezela
Iqhosha lokukhetha izinto.
Cinezela
Isitshixo sokuqalisa uvavanyo.
Cinezelaisitshixo umva kujongano lokuqala
4.1 Kolu nxibelelwano, cofa iqhosha lika-"Set", seta i-stiring speed kunye ne-Ext.ixesha.
Umfanekiso 6-5
Cofa isantya esishukumisayo (inxalenye yenombolo) ukuseta isantya esishukumisayo sesixhobo.Cofa i-Ext.ixesha (inxalenye yenombolo) ukuseta ixesha lokulibaziseka kwinqanaba lokugqibela lovavanyo.
Isantya esishukumisayo: Xa i-viscosity yesampula evavanyiweyo inkulu, isantya esishukumisayo sinokunyuswa ngokufanelekileyo.Kuxhomekeke ekubeni kungabikho amaqamza kwi-electrolyte eshukumisayo.
Ext.Ixesha: Xa kuyimfuneko ukwandisa ixesha lokuvavanya isampuli, njenge-solubility embi yesampuli kunye ne-electrolyte okanye ukuvavanya umxholo wamanzi wegesi, ixesha lokuvavanya linokwandiswa ngokufanelekileyo.(Qaphela: Xa ixesha le-Ext libekwe kwimizuzu eyi-0, uvavanyo lugqityiwe emva kokuba isantya se-electrolysis sesixhobo sizinzile. Xa ixesha le-Ext libekwe kwimizuzu emi-5, uvavanyo luqhubeleka kwimizuzu emi-5 emva kwesantya se-electrolysis. isixhobo sizinzile)
4.2 Emva kokuba ibhalansi yesixhobo igqityiwe, imeko yangoku iya kubonisa "Cofaisitshixo sokulinganisa". Ngeli xesha, isixhobo sinokulinganiswa okanye isampulu inokulinganiswa ngokuthe ngqo.
Ukulinganisa isixhobo, sebenzisa i-0.5ul sampler ukuthatha i-0.1ul yamanzi, cofa iqhosha elithi "Qala", kwaye ulitofe kwi-electrolyte nge-inlet yesampuli.Ukuba umphumo wokugqibela wokuvavanya uphakathi kwe-97-103ug (i-sampler engeniswa), ibonisa ukuba isixhobo sikwimeko eqhelekileyo kwaye isampuli inokulinganiswa.(Isiphumo sovavanyo lwesampulu yasekhaya siphakathi kwe-90-110ug, ebonisa ukuba isixhobo sikwimeko eqhelekileyo).
4.3 Isampulu yokubhalwa kweTitration
Xa isixhobo silinganisa (okanye silinganiswe), imeko yangoku "i-Titrating", ngoko isampuli inokulinganiswa.
Thatha isixa esifanelekileyo sesampulu, cinezela iqhosha elithi "Qala", faka isampuli kwi-electrolyte nge-inlet yesampuli, kwaye isixhobo siya kuvavanya ngokuzenzekelayo kude kube sekupheleni.
Qaphela: Umthamo wesampulu uncitshiswe ngokufanelekileyo okanye unyuswe ngokwengqikelelo yamanzi kwisampulu.Inani elincinci lesampulu lingathathwa kunye ne-50ul sampler ukuze kuhlolwe.Ukuba ixabiso lomxholo wamanzi elilinganisiweyo lincinci, umthamo wenaliti unokunyuswa ngokufanelekileyo;Ukuba ixabiso lomxholo wamanzi elilinganisiweyo likhulu, umthamo wenaliti ungancitshiswa ngokufanelekileyo.Kufanelekile ukugcina umphumo wokugqibela wokuvavanya umthamo wamanzi phakathi kwamashumi e-micrograms kunye namakhulu e-micrograms.Ioyile yeTransformer kunye neoyile ye-injini yomphunga inokutofwa ngokuthe ngqo kwi-1000ul.
5. Iziphumo zoMlinganiso
Emva kokuba uvavanyo lwesampula lugqityiwe, ifomula yokubala ingatshintshwa njengoko ifunwa, kwaye inombolo kwicala lasekunene lefomula yokubala ingatshintshwa phakathi kwe-1-5.(ihambelana ne-ppm, mg/L kunye ne-% ngokulandelelanayo)
Uluhlu lokulinganisa oluqhelekileyo lwesi sixhobo ngu-0μg-100mg.Ukuze ufumane iziphumo zovavanyo ezichanekileyo, isixa sesampulu etofiweyo kufuneka ilawulwe ngokufanelekileyo ngokomxholo wokufuma wesampulu yovavanyo.
1. Isampulu yolwelo
Umlinganiselo wesampulu yolwelo: isampulu evavanyiweyo kufuneka itsalwe ngesampulu yesitofu, emva koko itofwe kwigumbi le-anode yeseli ye-electrolytic ngezibuko lenaliti.Phambi kokutofa kwesampulu, inaliti kufuneka icocwe ngephepha lokucoca.Kwaye incam yenaliti kufuneka ifakwe kwi-electrolyte ngaphandle kokunxibelelana ne-inwall yeseli ye-electrolytic kunye ne-electrode xa isampuli yovavanyo itofwa.
2. Isampulu eqinileyo
Isampulu eqinileyo inokuba kuhlobo lomgubo, isuntswana okanye ibhloko yemess (ibhloko enkulu kufuneka icudiwe).I-evaporator yamanzi efanelekileyo iya kukhethwa kwaye idibaniswe kwisixhobo xa isampuli yovavanyo inzima ukuchithwa kwi-reagent.
Ukuthatha isampulu eqinileyo enokuthi inyibilikiswe kwi-reagent njengomzekelo wokuchaza naliti yesampulu eqinileyo, ngolu hlobo lulandelayo:
Umfanekiso 7-1
I-1) I-injector yesampuli eqinile iboniswa njengomfanekiso we-7-1, yihlambulule ngamanzi kwaye yomise kakuhle.
2) Thatha phantsi isiciko se-injector yesampuli eqinileyo, isampuli yokuvavanya isampuli, gubungela isiciko kwaye ulinganise ngokuchanekileyo.
3) Thatha phantsi iqhude leplagi ye-electrolytic cell sample injection port, faka i-injector yesampuli kwi-injection port ngokomgca opheleleyo oboniswe njengomfanekiso 7-2.Jikelezisa isampulu yesampulu eqinileyo ye-injector yeedigri ze-180 eboniswe njengomgca onamachaphaza kumfanekiso 7-2, wenze isampuli yovavanyo ihla kwi-reagent de umlinganiselo uphele.Kwinkqubo yayo, isampulu yovavanyo oluqinileyo ayinakuqhagamshelwana ne-electrolytic electrode kunye ne-electrode elinganisiweyo.
Umfanekiso 7-2
Ukulinganisa isampuli ye-injector kunye nesivalo ngokuchanekileyo kwakhona emva kokutofa.Umgangatho wesampuli unokubalwa ngokomahluko phakathi kwemilinganiselo emibini, engasetyenziselwa ukubala umlinganiselo womthamo wamanzi.
3. Isampulu yegesi
Ukuze ukufuma kwirhasi kunokufunxwa yi-reagent, isidibanisi siya kusetyenziswa ukulawula isampulu yovavanyo ukuba itofwe kwiseli ye-electrolytic nangaliphi na ixesha. (jonga umfanekiso 7-3).Xa ukufuma kwisampulu yovavanyo lwegesi kulinganiswa, i-reagent emalunga ne-150ml kufuneka itofwe kwiseli ye-electrolytic ukuqinisekisa ukuba ukufuma kunokufunxwa ngokupheleleyo.Ngexesha elifanayo, ukuhamba kwegesi kuya kulawulwa kwi-500ml ngomzuzu.malunga.Kwimeko apho i-reagent inciphisa ngokucacileyo kwinkqubo yokulinganisa, malunga ne-20ml glycol kufuneka ifakwe njengesongezelelo.(ezinye i-reagent yeekhemikhali zingongezwa njengesampulu elinganisiweyo yokwenyani.)
Umfanekiso 7-3
A. Ugcino
1. Zigcine kude nelanga, kwaye ubushushu begumbi kufuneka bube phakathi kwe-5℃～35℃.
2. Musa ukuyifaka kwaye uyisebenze phantsi kokusingqongileyo ngokufuma okuphezulu kunye nokuguquguquka okukhulu konikezelo lwamandla.
3. Musa ukuyibeka kwaye uyisebenze phantsi kokusingqongileyo ngerhasi eyonakalisayo.
B. Ukutshintshwa kwe-silicone pad
Iphedi yesilicone kwizibuko lesampulu yokutofa kufuneka itshintshwe kwangexesha ngenxa yokuba ukusetyenziswa kwayo ixesha elide kuya kwenza umngxuma wokuqhotsa ungathinteli kwaye uvumele ukufuma kungene, okuya kuba nefuthe kumlinganiselo. (jonga umfanekiso 4-4)
1. Ukutshintshwa kwe-silicagel ye-allochroic
I-silicagel ye-allochroic kumbhobho wokomisa kufuneka itshintshwe xa umbala wayo ujika uluhlaza okwesibhakabhaka ukusuka eluhlaza okwesibhakabhaka.Musa ukubeka i-silicagel powder kwipayipi yokumisa xa utshintsha, ngaphandle koko ukukhutshwa kweseli ye-electrolytic kuya kuvinjelwa kubangele ukupheliswa kwe-electrolysis.
2. Ukugcinwa kwe-electrolytic cell polishing port
Jikelezisa izibuko lokupholisha leseli ye-electrolytic rhoqo ngeentsuku ezisi-7-8.Nje ukuba ingakwazi ukujikeleziswa ngokulula, gcoba ngegrisi yokufunxa kancinci kwaye uyifake kwakhona, kungenjalo kunzima ukuyikhulula ukuba iiyure zenkonzo zinde kakhulu.
Ukuba i-electrode ayinakuthatyathwa phantsi, nceda ungayikhuphi ngaphandle ngenkani.Ngalo mzuzu, ukuba nkxu yonke iseli electrolytic emanzini afudumeleyo iiyure 24-48 rhoqo, emva koko ukuyisebenzisa.
3. Ukucocwa kweeseli ze-electrolytic
Vula yonke imiphetho yebhotile yeglasi yeseli ye-electrolytic.Coca ibhotile yeseli ye-electrolytic, umbhobho wokomisa, iplagi yokutywina ngamanzi.Yomise kwi-oveni (ubushushu be-oveni bumalunga ne-80 ℃) emva kokucoca, emva koko uyipholise ngokwendalo.I-alcohol ethyl epheleleyo ingasetyenziselwa ukucoca i-electrolusis electrode, ngelixa amanzi engavumelekanga.Emva kokucoca, yomise ngesomisi.
Qaphela: Musa ukucoca i-electrode lead, njengoko kubonisiwe umfanekiso 8-1
Umfanekiso 8-1
C. Faka esikhundleni se-Electrolyte
1. Thatha i-electrolytic electrode, i-electrode yokulinganisa, ityhubhu yokomisa, iplagi yokutofa kunye nezinye izincedisi kwibhotile yeseli ye-electrolytic.
2. Susa i-electrolyte ukuba ithathelwe indawo kwibhotile yeseli ye-electrolytic.
3. Coca ibhotile yeseli ye-electrolytic, i-electrolytic electrode kunye ne-electrode yokulinganisa nge-ethanol epheleleyo.
4. Yomisa ibhotile yeseli ye-electrolytic ecociweyo, i-electrolytic electrode, njl. kwi-oven engekho ngaphezulu kwe-50℃.
5. Galela i-electrolyte entsha kwibhotile yeseli ye-electrolytic, kwaye ugalele isixa esimalunga ne-150ml (phakathi kwemigca emibini ethe tye emhlophe yebhotile yeseli ye-electrolytic).
6. Faka i-electrolytic electrode, i-electrode yokulinganisa, kunye neplagi yesampuli ye-tube eyomileyo, njl., kwaye ugalele i-electrolyte entsha kwi-electrolyte electrode, isixa esithululwayo siyafana nenqanaba lolwelo lwe-electrolyte kwibhotile yeseli ye-electrolytic.
7. Faka i-layer ye-vacuum grease kuzo zonke izibuko zokugaya zeseli ye-electrolytic (i-electrolytic electrode, i-electrode yokulinganisa, i-injection plug, iplagi yokugaya iglasi).
8. Beka ibhotile yeseli ye-electrolytic endaweni ye-electrolytic cell clamp yesixhobo, kwaye ujike isixhobo kwisimo se-titration.
9. I-reagent entsha kufuneka ibe bomvu-mdaka kwaye ikwimeko ye-iodine.Sebenzisa i-50uL yokutofa malunga ne-50-100uL yamanzi de i-reagent ijike ibe tyheli.
1. Akukho mboniso
Unobangela: Intambo yamandla ayiqhagamshelwanga;iswitshi yamandla ayidibanisi kakuhle.
Unyango: Qhagamshela intambo yombane;buyisela iswitshi yamandla.
2. Vula isiphaluka sokulinganisa i-electrode
Isizathu: I-electrode yokulinganisa kunye neplagi yesixhobo ayixhunyiwe kakuhle;ucingo lokudibanisa lwaphukile.
Unyango: Qhagamshela iplagi;buyisela intambo.
3. I-Electrolysis velocity ihlala i-zero ngexesha le-electrolysis.
Isizathu: I-electrolytic electrode kunye neplagi yesixhobo ayixhunyiwe kakuhle;ucingo loqhagamshelwano lwaphukile.
Unyango: Qhagamshela iplagi;buyisela intambo.
4. Isiphumo sokulinganisa samanzi acocekileyo sincinci, xa isampuli yovavanyo ifakwe, ayinakufunyanwa ngesixhobo.
Unobangela: I-electrolyte ilahlekelwa ukusebenza kakuhle.
Unyango: Faka esikhundleni se-electrolyte entsha.
5. Inkqubo ye-Electrolytic ayinakuphela.
Unobangela: I-electrolyte ilahlekelwa ukusebenza kakuhle.
Unyango: Faka esikhundleni se-electrolyte entsha.
